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Beilstein J. Org. Chem. 2018, 14, 2737–2744, doi:10.3762/bjoc.14.252
Graphical Abstract
Scheme 1: Targeted conversion of CNSL into a tyrosinase inhibitor.
Scheme 2: Previous synthesis of 2-hydroxy-6-tridecylbenzoic acid by Fu et al.
Scheme 3: Ethenolysis of the crude CNSL.
Figure 1: State-of-the-art metathesis catalysts.
Scheme 4: Overall process in a preparative scale.
Beilstein J. Org. Chem. 2010, 6, No. 43, doi:10.3762/bjoc.6.43
Scheme 1: Proposed mechanism for the decarboxylative Heck reaction.